Pure phase Y
3Fe
5O
12 (YIG) ceramic was successfully produced by
tape-casting forming process and one-step solid-state sintering method. The activation energy for densification was
calculated to be 183.81 kJ/mol. Pure YIG ceramic with a relative density as high as 99.8% was fabricated. The existence
of O vacancy and Fe
2+ ions was determined by XPS and EPR spectra.
The RT saturation magnetization was measured to be 28.2 emu/g, and the hysteresis
loss was calculated to be smaller than 10 mJ/kg in the temperature range of 230~360 K and be as high as 238.8 mJ/kg at 30 K. The
dielectric loss tangent tan
δε was nearly zero
at 6~7 GHz and 11~12
GHz. For complex permeability in the frequency range
of 5~18 GHz, the magnetic loss
tangent tan
δμ fluctuated
at around zero. Therefore, the low values of tan
δε and tan
δμ indicate that it is a low loss ceramic
material.